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14315-16-3 3-aminobenzanilide

product Name 3-aminobenzanilide
CAS No 14315-16-3
Molecular Formula C13H12N2O
Molecular Weight 212.2472
InChI InChI=1/C13H12N2O/c14-11-6-4-5-10(9-11)13(16)15-12-7-2-1-3-8-12/h1-9H,14H2,(H,15,16)
EINECS 238-257-8
Molecular Structure 14315-16-3 3-aminobenzanilide
Density 1.244g/cm3
Boiling point 323.9°C at 760 mmHg
Refractive index 1.688
Flash point 149.7°C
Vapour Pressur 0.000254mmHg at 25°C

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Specifications 99% min
Packing 25kg 50kg drum or bag
Description What is the chemical of 3-Aminobenzanilide ? Appearance: Light yellow to yellow solid£» Assay:99%min by HPLC£» IR Identity: conform to standard£» HNMR£º conform to standard£» carbon spectrum: conform to standard£» Water by K. F.:0.5% max or as per the customer¡¯s request£» Loss on drying:0.5% max. or as per the customer¡¯s request£» =============================================================================== Overview of Synthesis Methods: Raw Material Preparation: N-(3-nitrophenyl)benzamide is used as the starting material, which can be prepared by acylation reaction of benzoyl chloride with m-nitroanil-ine. Reduction Reaction: Dissolve N-(3-nitrophenyl)benzamide in solvents such as ethanol, add a reducing agent (e.g., iron powder, aqueous ammonium chloride solution), and reflux under heating. This method belongs to the classic iron powder-acid reduction method, which is suitable for selective reduction of nitro groups and has minimal impact on amide groups. The reaction equatio...
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